WDX spectrometers attached to the electron microprobe

Electron microprobe

WDX spectrometers attached to the electron microprobe
Foto: Stefan Kiefer

General information

All natural and synthetic solid bodies are defined by their chemical composition. The electron microprobe is an instrument that allows accurate and precise determination of chemical composition with micrometer resolution. It is possible to measure and visualize variations in the chemical composition in selected areas of the samples. The electron-optical technology in this instrument allows for correlation of solid-state properties and chemical composition in µm-range. An electron microprobe is an excellent choice for reproducible, highly accurate analytical results that find their use in geosciences, chemistry, physics, materials chemistry in academia, industry, and government institutions.

The electron microprobe can be used for

  • quantitative and qualitative analyses of major, minor, and trace elements (> 100ppm / 0.01 wt.%)
  • analyses of all elements from oxygen to uranium in solid samples
  • visualization of the surface of the sample (back-scattered and secondary electron images, cathodoluminiscence)
  • creation of element distribution maps and concentration profiles

JEOL JXA-8230 electron microprobe

Foto: Stefan Kiefer
  • Advantages and sample formats

    Advantages and sample format

    The greatest advantage of the method is the possibility of non-destructive analysis of small sample volumes in µm-range

    Samples

    • standard thin and polished sections
    • thin sections with dimensions of 28 x 48 mm
    • round polished section with diameter of 1'' (25.4 mm)
    • round polished sections with diameter not larger than 30 mm
    • for non-standard sample formats, contact us and we will find a solution möglich

    The surface of the sample must be polished and clean. Before the measurement, the samples will be coated with a thin layer of carbon.

     

    Sample holder for three thin sections and six polished sections

    Foto: Stefan Kiefer
  • Excerpt from the user regulations

    Im Auszug der Nutzerordung EPMApdf, 838 kb sind Ausstattungsinformationen, mögliche Entgelte sowie weitere Informationen enhalten.

Contact information

Stefan Kiefer, Dr.

Stefan Kiefer
Foto: Stefan Kiefer